Chemistry 24 - Dr. Kline

Course Information

Reference

Chemistry Lab Safety Rules | Information
Avoiding Plagiarism
Collaboration - when you may and may not work with others
Lab Techniques |OChem.com (→ In The Lab)
Spectroscopy Tables - NMR and IR

Experiment	Report Sheet \| due date*	Other Information
Butyl Benzoate (18M)	Report PDF \| 3/12/09	You want the actual Miniscale procedure that starts on page 29, not the one that is microscale, but labeled as miniscale!
Alkylation of 1,4-Dimethoxybenzene (22m)	Report PDF \| 3/26/09
Synthesis of Para Red (Handout)	Report PDF \| 4/02/09	Background, Procedure, etc. in Handout linked at left; Essay on Dyes and Dyeing in .NExT due to copyright restrictions
Synthesis of Benzoylamino Acids (28.1m)	Report PDF \| 4/23/09	Each pair will be assigned an amino acid: glycine, alanine, or valine.
Synthesis and Identification of an Ester (12.1m)	Report PDF \| 4/30/09	List of Alcohols from Shriner (class handout); List of Alcohols from Mohrig (go to "Appendix and look for table of alcohols). List of possible alcohols, with bp's, should be listed in NB before lab.
Grignard Synthesis of 1,1-Diphenylethanol (15.1M, 15.2M)	Report PDF \| 5/11/09	Diagram of apparatus (replaces Figure 7.2a in Techniques book)
Synthesis of 4-tert-Butylcyclohexanone (by oxidation of the alcohol) (Project 4.1M)	Report PDF \| 5/14/09	Will take IR of product (week following experiment); IR spectra of starting material and product online via eCompanion.
Synthesis of 4-tert-Butylcyclohexanol (by reduction of the above ketone) (Project 4.2m)	Report PDF \| 5/21/09	Will take proton NMR of product (week following experiment).
Aldol Dehydration (Project 11.1M)	Report PDF \| 5/28/09	Students will be assigned different combinations of starting materials; need mp data for all possible products in Notebook before lab.
Organic Qualitative Analysis - General Unknown (Handout)	Preliminary Report PDF \| due when you want spectra Final Report PDF \| 6/11/09	Handout; Mohrig Text Website has information, procedure, etc. Look for "Part IV: Qualitative Organic Analysis." You need both the procedure (Techniques) and the tables of compounds (Appendix). This is a solo experiment.
Organic Qualitative Analysis - Carbohydrate (Handout)	Report PDF \| 6/11/09	Handout, including table of possible unknowns. This is a solo experiment.

* Note -if due date is still listed in 2007, Report PDF may not be the correct version. Be sure to use the most current version when submitting lab reports.

Last Revised 05/17/2009